Progress of Solid-Phase Microextraction Coatings and Coating Techniques
نویسندگان
چکیده
منابع مشابه
Carbon nanocones/disks as new coating for solid-phase microextraction.
In this article, the potential of carbon nanocones/disks as coating for solid-phase microextraction has been evaluated for the first time. The nanostructures were immobilized on a stainless steel needle by means of an organic binder. The fiber coating obtained was ca. 50 microm of thickness and 35 mm in length. The evaluation of the sorbent capacity was carried out through the determination of ...
متن کاملSolid phase microextraction.
Solid Phase Microextraction (SPME) uses a small volume of sorbent dispersed typically on the surface of small fibres, to isolate and concentrate analytes from sample matrix. After contact with sample, analytes are absorbed or adsorbed by the fibre phase (depending on the nature of the coating) until an equilibrium is reached in the system. The amount of an analyte extracted by the coating at eq...
متن کاملTheory of solid-phase microextraction
The main objective of this contribution is to describe the fundamental concepts associated with solid-phase microextraction (SPME). Theory provides insight when developing SPME methods and identifies parameters for rigorous control and optimization. A mathematical model has been developed to understand the principal processes of SPME by applying basic fundamental principles of thermodynamics an...
متن کاملLaser Desorption Solid Phase Microextraction
The use of laser desorption as a sample introduction method for solid-phase microextraction (SPME) has been investigated in this research project. Three different types of analytical instruments, mass spectrometry (MS), ion mobility spectrometry (IMS) and gas chromatography (GC) were employed as detectors. The coupling of laser desorption SPME to these three instruments was constructed and desc...
متن کاملPowdery polymer and carbon aerogels with high surface areas for high-performance solid phase microextraction coatings.
A novel powdery polymer aerogel (PPA) with a hierarchical pore structure was prepared via hypercrosslinking of monodisperse poly(styrene-co-divinylbenzene) nanoparticles. Subsequently, the PPA was carbonized to obtain a powdery carbon aerogel (PCA) with a well-inherited pore structure and a much higher surface area (2354 m2 g-1). The PPA-coated and PCA-coated fibers were easily fabricated benef...
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ژورنال
عنوان ژورنال: Journal of Chromatographic Science
سال: 2006
ISSN: 0021-9665,1945-239X
DOI: 10.1093/chromsci/44.6.324